Aspend simulation software and laboratory model were used to study the recovery technology of extractant methanol in glycine production process. Two paths were designed : on the one hand, methanol in glycine centrifugal mother liquor was recovered ; on the other hand, the methanol in the tail gas of glycine drying was recovered. It has been proved in the laboratory that the methanol content produced by the distillation column is≥98.5% and the energy consumption is the lowest when the packed distillation column is used, the preheating temperature is 60 ℃ and the reflux ratio is 0.5. The method of condensation-water absorption-desorption-molecular sieve absorption can also absorb methanol in glycine drying exhaust gas to the maximum extent, thus further reducing methanol consumption.
赵柯柯,王青青,王玉琪,李桂平,赵晓燕,张振友. 甘氨酸生产过程中甲醇回收技术研究[J]. 煤炭与化工, 2026, 49(9): 134-137,160.
Zhao Keke, Wang Qingqing, Wang Yuqi, Li Guiping, Zhao Xiaoyan, Zhang Zhenyou. Study on methanol recovery technology in glycine production process. CCI, 2026, 49(9): 134-137,160.