Parapropanol was synthesized from p-aminophenol and propionic acid. with activated carbon as decolorizing agent and sodium pyrosulfite as antioxidant. The effects of different reaction conditions, such as molar ratio of raw materials, reaction time and reaction temperature on the yield were studied. Experimental results showed that when p-aminophenol and propionic acid molar ratio was 1∶1.3, reaction temperature was 110 ℃, reaction time was 3 h, the parapropanol yield was up to 90%. The structure of the product was characterized by melting point determination and liquid chromatography analysis, the purity was 98.7%.
马宁宁1，刘晓莲1，郝新庭1，刘向军2，魏蒙蒙1，李红仓3. 对丙胺酚合成工艺研究[J]. 煤炭与化工, 2020, 43(8): 138-139,142.
Ma Ningning1, Liu Xiaolian1, Hao Xinting1, Liu xiangjun2， Wei mengmeng1, Li Hongcang3. Research on synthesis of parapropanol. CCI, 2020, 43(8): 138-139,142.
