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| Research and application of anticorrosion technology for high pressure reaction water condenser of nitric acid |
| Cai Xiaoliang |
| Tangshan Zhonghao Chemical Corporation Ltd., Tangshan 063611, China |
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Abstract Aiming at the problems such as leakage of high-pressure reactive water condenser caused by long-time operation in nitric acid production process of double pressure method, emergency interlock shutdown of nitric acid plant, serious corrosion of downstream equipment and circulating water pipe network caused by the leakage nitrogen oxide gas, and pollution environment caused by the leakage of nitrogen oxide gas, the corresponding treatment measures were put forward. Through analyzing the causes of leakage, the preventive measures such as reducing the amount of dilute acid, reforming the exhaust pipeline, regular cleaning, monitoring the quality of circulating water, upgrading the material of condenser and increasing distributor were further put forward, which effectively solved the problem of frequent leakage of high pressure reactive water condenser, and ensured the safe and stable operation of nitric acid unit.
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| [ 1 ] 赵小燕,刘希武,崔新安,等. 304L不锈钢在稀硝酸环境下的腐蚀研究[ J ]. 中国腐蚀与防护学报,2018,38( 5 ):455 - 462.
[ 2 ] 杨 健,董永明. 高压反应水冷凝器列管泄漏原因分析及处理[ J ]. 化学工程与装备,2016( 7 ):174 - 176.
[ 3 ] 潘旭东,王向明. 循环水中氯离子控制及对不锈钢腐蚀机理探讨[ J ]. 工业水处理,2013( 3 ):14 - 20.
[ 4 ] 卢日时,李 刚. 316、317耐氯离子腐蚀能力浅析[ J ]. 机械工程师, 2013( 6 ):246 - 247.
[ 5 ] 左景伊. 腐蚀数据与选材手册[ M ]. 北京:化学工业出版社,2004.
[ 6 ] 刘莺歌. 高压反应水冷凝器有限元应力分析[ J ]. 山东化工,2018( 24 ):99 - 100.
[ 7 ] 林玉珍,杨德钧. 腐蚀与腐蚀控制原理[ M ]. 北京:中国石化出版社,2007.
[ 8 ] 金 燕,桑芝富,汤成亮. 硝酸装置冷凝器的换热管与管板内孔全对接焊的实施[ J ]. 化工设备与管道,2004,41( 6 ):57 - 59.
[ 9 ] 蔡仁孔. 提高换热器管板与管子连接接头质量浅谈[ J ]. 化工设备与管道,2000,37( 2 ):14 - 15.
[ 10 ] 刘振宏. 硝酸生产装置腐蚀原因分析及防护对策[ J ]. 石油化工设备技术,2006,27( 6 ):61 - 64. |
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